СРАВНИТЕЛЬНЫЙ АНАЛИЗ АНАЛИТИЧЕСКИХ МЕТОДОВ ОПРЕДЕЛЕНИЯ АЛЛОХТОННОГО ОРГАНИЧЕСКОГО ВЕЩЕСТВА НЕФТЕЗАГРЯЗНЕННЫХ ПОЧВ
DOI:
https://doi.org/10.24852/2411-7374.2024.1.57.66Ключевые слова:
нефтяное загрязнение, серые лесные почвы, инфракрасная спектроскопия, газовая хроматография, гравиметрия, потеря массы при прокаливанииАннотация
Проведен сравнительный анализ четырех аналитических методов (инфракрасная спектрометрия, газовая хроматография, гравиметрия, потеря массы при прокаливании) определения концентрации аллохтонных соединений на примере серой лесной почвы, загрязненной разными дозами нефти. Измерения проводили через сутки и 90 дней после загрязнения. Показано, что количественные данные формируемого аналитического сигнала сильно разнятся, поскольку зависят от специфики используемого метода, начального уровня нефтяного загрязнения и времени выветривания. Результативность рассматриваемых методов можно расположить в следующем порядке: потеря при прокаливании > гравиметрия > газовая хроматография > инфракрасная спектрометрия. Для более корректной оценки содержания органических соединений нефти, изменения его фракционного состава предлагается совместное использование различных аналитических инструментов
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